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1200℃ Ultrasonic Atomization And Continuous Collection Thermal Decomposition Vertical Furnace

  • Model Number:

    TMAX-1200VF
  • Compliance:

    CE certificate
  • Warranty:

    One year limited warranty with lifetime technical support
  • Payment:

    T/T, Credit Card, Paypal, LC, Western Union
  • Delivery Time:

    3 days
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DESCRIPTION

1200℃ Ultrasonic Atomization And Continuous Collection Thermal Decomposition Vertical Furnace


A.Overview

Ultrasonic atomization and continuous collection thermal decomposition vertical furnace uses low ultrasonic vibration energy to atomize liquid. The liquid can be delivered to the spray head by its own gravity or a low-pressure liquid pump to achieve continuous or intermittent atomization and react in the high temperature zone. Typical applications Thin film spraying (solar cell, fuel cell, touch screen, flux, glass spray film, etc.. It can also be used for nano synthesis. The synthesized nanoparticles brought by flowing gas and free sedimentation can be effectively collected in stainless steel tanks.

 

B.Specification

Type

Ultrasonic atomization and continuous collection thermal decomposition vertical furnace

Equipment composition

1. Atomization device: equipped with a 2.4MHz ultrasonic atomizer, which can atomize the liquid into liquid particles, and then introduce them into the tube furnace. The ultrasonic atomizer is connected to a stainless steel liquid collection tank to ensure that the liquid that is not atomized will not enter the tube furnace.

2. Liquid flow control device: constant flow pump

3. Heating part (tube furnace): the maximum temperature of the tube furnace can reach 1200℃.

4. Nano powder continuous collection device: the diameter of the collection tank is 60mm, which can effectively collect the nanoparticles brought by the flowing gas and free sedimentation. There is a flap valve on the collection tank. When the tank is full, the flap valve can be closed.

Atomization equipment

Atomization equipment

1. 220VAC, 2.4 MHz ultrasonic generator

2. Fluoropolymer coated liquid container and fluoropolymer sealing gasket

3. External fluoropolymer optical sensor and valve to keep the liquid level at the correct height

4. Ultrasonic power is programmable, 0~100%, increment of 5%.

5. 316L stainless steel T-piece, equipped with dia6mm PTFE tank card sleeve joint, can use PTFE tube to carry gas.

Nano continuous collection device

The diameter of the collection tank is 60mm, which can effectively collect the nanoparticles brought by flowing gas and free sedimentation. There is a flap valve on the collection tank. When the tank is full, you can close the flap valve, open the card sleeve, and pour out the nano particles. The particles are then connected with a ferrule, the canister is vacuumed, and the valve is opened to continue collecting.

Power

2.5KW

Tube size (OD, mm)

Dia 60(OD) X1300 mm

Dimension(L*D*H)

800X500X2000

Supply voltage

220V

Phase

Single phase

Heating element

Domestic high-quality resistance wire (optional Kanthal A1 imported resistance wire)

Temperature control

 

UAV  program temperature control instrument (standard)

1.30 - stage program temperature control intelligent PID adjustment.

2.With over-temperature protection, the electric furnace heating circuit is automatically cut off when the temperature is over-temperature or broken, (when the electric furnace temperature exceeds 1200 degrees or the thermocouple is blown, the AC relay on the main circuit will be automatically disconnected, the main circuit is broken. On, the ON light on the panel is off, the OFF light is on, and the limited protection electric furnace).

3. With 485 communication interface (standard when purchasing software)

4. With power-off protection function, that is, when the power is turned on after the power is turned off, the program does not start from the starting temperature, but the furnace temperature rises from the time of power failure.

5. The meter has the function of temperature self-tuning

tube furnace


If you want to get an imported temperature controller, you may have the following choices for replacement with extra fees.

tube furnace 


Tube Furnace Materials

1. High-quality and high-purity alumina polycrystalline fiber curing furnace formed by vacuum suction filtration.

2. It is formed by Japanese technology.

3. The spacing and pitch of the resistance wires in the furnace are all arranged according to the best thermal technology in Japan, and the temperature field is simulated by thermal software

Control accuracy

 +/- 1 ℃

Trigger

Phase-shifted trigger

Electric appliance

Zhejiang chint

Silicon controlled

106/16E SEMIKRON

Maximum temperature

First temperature zone:1200℃

Second temperature zone:1200℃

Third temperature zone:1200℃

Rated temperature

First temperature zone:1100℃

Second temperature zone:1100℃

Third temperature zone:1100℃

Heating rate

≤30 ℃/ Min (it can be modified as required)

Recommended rate of temperature rise

≤15  ℃/ Min

Thermocouple Type

K Type

Heating length

420mm

Peripheral surface temperature

≤45℃

Open cover protection system

When the furnace cover is opened, the relay will automatically cut off the main power supply, effectively ensuring the safety of the user.

Vacuum system (optional)

tube furnace

1) Generally, the gas in the furnace tube can be pumped out by roughly vacuumizing:TW-1.5A single-stage pump would be fine

2)  The double-stage pump 2XZ-2 vacuum pump can pump the vacuum degree of tube furnace tube to about 10Pa.

3) The VS-0.1 vacuum system can pump the vacuum degree in the tube furnace to 0.1Pa (with resistance vacuum meter display).

4) VS high vacuum system (composed of molecular and mechanical pump) can pump the vacuum degree in the tube furnace to 10-3 Pa.

5) Constant pressure pump (the system can control the pressure in the pipe within - 100.0KPa ~ 100.0KPa).

6)  British (INFICON) capacitance vacuum gauge (measuring range: 3.8x10-5 -1125 Torr, it can detect various gases, including mixed gases, with accurate measurement, good repeatability, and optional anti-corrosion type: PCG554)

Vacuum flange at the bottom

1. In order to increase the pumping rate and achieve higher vacuum requirements. The original hose connector can be replaced with KF-25 interface (VS-0.1 and VS high vacuum system interfaces are both KF25)

2. If used in the air supply system, the original hose connector can be replaced with a Φ6.35mm double ferrule connector.

Upper vacuum flange

 upper vacuum flange

Gas supply system

(Optional)

gas supply system




C.Precautions

1. The gas pressure in the furnace tube can not be higher than 0.02MPa

2. Since the internal pressure of the cylinder is high, when the gas is introduced into the furnace tube, a pressure reducing valve must be installed on the cylinder. To ensure safety, it is recommended to use a pressure lower than 0.02 MPa.

3. When the furnace tube used is a corundum tube, when the furnace temperature is higher than 1500 °C, the furnace tube should not be in a vacuum state, and the gas pressure in the furnace tube should be equivalent to the atmospheric pressure.

4. The gas flow into the furnace tube should be less than 200SCCM to avoid the impact of cold air flow on the hot furnace tube.

5. For the sample heating experiment, it is not recommended to close the suction valve and intake valve at the flange end of the furnace tube. If you need to close the air valve to heat the sample, you should always pay attention to the pressure gauge. If the air pressure is greater than 0.02 MPa, you must open the exhaust valve immediately to prevent accidents (such as furnace tube rupture, flange flying out, etc.)

6. Do not use graphite crucible in alumina tubes

7. MoSi2 heating element must not be used for a long time at low temperature (400 ° C - 700 ° C), otherwise it may damage the heating element

tube furnace


 

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